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PF-06873600-LCMS-36714-MedChemExpress

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MS Report from Instrument: LCMS-02 File ..1\\DATA\\2019\\20190111\\544\\BIZ2019-110-CXL2.D Tgt Mass (CHM): Injection Date : 11 Jan 19 10:20 am +0800 Seq. Line : 13 Sample Name : BIZ2019-110-CXL2 Location : P2-D-09 Acq. Operator : LQ_1052 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\data\\2019\\20190111\\544\\1-POS-3MIN-1.M Analysis Method : D:\\CHEM32\\1\\DATA\\2019\\20190111\\544\\1-POS-3MIN-1.M Catalog No : HY-114177 Batch#36714 BY ACN Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-314 Oven Temperature : 45󰀀 DAD1 B, Sig=214,4 Ref=off 10001.25450000.5 DAD1 C, Sig=254,4 Ref=off mAU2001.5381.26010000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701000008000060000400002000000.511.5 Ion 472.2, MSD1 472.2,Target Mass 471.2 +H Positive, EIC=471.9:472.9 4000030000200001000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.71111.660mAU1.51.66022.5min1.7111.51.71022.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.25 0.01 0.35 0.65 0.02 ND 1.66 0.02 1482.41 13. 99.98 472 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.26 0.01 0.06 0.16 0.02 ND 1.54 0.02 0.63 0.47 0.21 ND 1.66 0.02 300.52 282.14 99.71 472 1.71 0.01 0.19 0.35 0.06 472 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.71 0.04 286336.25 101755.18 100.00 472LCMS-02 1/11/2019 10:27:03 LQ_1052

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MS Report from Instrument: LCMS-02

Ret. Time: 1.71 <<<< POSITIVE SPECTRA >>>> ES-API Positive 472.2 454.2 455.2 474.1 473.1 494.1LCMS-02 1/11/2019 10:27:03 LQ_1052

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