Data File D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.DSample Name: CPK2015-708-03156=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 52Acq. Instrument : HY-LCMS-02 Location : P2-F-04Injection Date : 7/8/2015 3:10:23 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 7/8/2015 10:25:03 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\30-500MS+3MIN-1.5_(0.02%FA).MLast changed : 7/9/2015 11:10:04 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:30-500,Column ID:A-RP-134,40℃ Catalog No : HY-50877 Batch#03156 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.D) 1.699 1.853mAU800600400 1.961 2.075 2.39520000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.699 MF 0.0555 3488.17090 1048.24121 99.4690 2 1.853 FM 0.0319 6.75695 3.53478 0.1927 3 1.961 MM 0.0527 6.17918 1.95284 0.1762 4 2.075 MM 0.0378 2.76725 1.22015 0.07 5 2.395 MM 0.0446 2.91717 1.09055 0.0832 Totals : 3506.79146 1056.03953 ===================================================================== *** End of Report ***HY-LCMS-02 7/9/2015 11:10:08 AM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.DSample Name: CPK2015-708-03156=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 52Acq. Instrument : HY-LCMS-02 Location : P2-F-04Injection Date : 7/8/2015 3:10:23 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 7/8/2015 10:25:03 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\30-500MS+3MIN-1.5_(0.02%FA).MLast changed : 7/9/2015 11:11:50 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:30-500,Column ID:A-RP-134,40℃ Catalog No : HY-50877 Batch#03156 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.D) ES-API, Pos, Sc100000080000060000040000020000000.511.522.53min 1.708 HY-LCMS-02 7/9/2015 11:11:53 AM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.DSample Name: CPK2015-708-03156MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.708 5498410 545.20 I 544.20 I 372.10 I 272.60 I*MSD1 SPC, time=1.6:1.744 of D:\\AGLIENT 1260\\DATA\\20150708\\20150708 2015-07-08 10-25-03\\CPK2015-708-03156.D ES-API 272.6100806040200100200 544.2Max: 323728 372.1 546.2 545.2300400500600700m/z *** End of Report ***HY-LCMS-02 7/9/2015 11:11:53 AM Li Shan(LCMS-02)Page 2 of 2
