MS Report from Instrument: LCMS-03 File ..ata\\20171207\\20171207-1\\CPK2017-D05-09995.D Tgt Mass (CHM): Injection Date : 7 Dec 17 1:01 pm +0800 Seq. Line : 38 Sample Name : CPK2017-D05-09995 Location : P1-A-07 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171207\\20171207-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171207\\20171207-1\\1-POS-3MIN.M Catalog No : HY-13032 Batch#09995 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.6351.513mAU400200000.5 DAD1 B, Sig=254,4 Ref=offmAU1.528200000.5 ELS1 A, ELSD SignalmV1005000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.51.66922.5min112.1052.1551.51.63522.5min1.8101.51.70522.5min2000000000.511.5 Ion 424.9, MSD1 424.9,Target Mass 423.9 +H Positive, EIC=424.6:425.61.66622.5min200000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.51 0.03 1.38 0.46 0.14 233 1. 0.02 959.40 737.27 99.74 424 2.11 0.02 0.12 0.12 0.01 233 2.16 0.02 0.96 0.75 0.10 233 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.53 0.03 0.38 0.24 0.07 233 1. 0.02 513.93 394.12 99.85 424 1.81 0.03 0.37 0.22 0.07 233 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.67 0.06 16173445.00 3994822.25 100.00 424LCMS-03 12/7/2017 15:31:00 ZLJ_587Page1 of3MS Report from Instrument: LCMS-03Ret. Time: 1.67 <<<< POSITIVE SPECTRA >>>> ES-API Positive400000350000300000250000200000150000100000427.2500000100200300400500600700800900m/z873.3425.2871.2424.2LCMS-03 12/7/2017 15:31:00 ZLJ_587Page2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 12/7/2017 15:31:00 ZLJ_587Page3 of3
