MS Report from Instrument: LCMS-03 File ..ata\\20171207\\20171207-1\\CPK2017-D07-08402.D Tgt Mass (CHM): Injection Date : 7 Dec 17 8:17 pm +0800 Seq. Line : 128 Sample Name : CPK2017-D07-08402 Location : P1-E-06 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171207\\20171207-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171207\\20171207-1\\1-POS-3MIN.M Catalog No : HY-10809 Batch#08402 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off500250000.5 DAD1 B, Sig=254,4 Ref=offmAU400200000.5 ELS1 A, ELSD SignalmV200100000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70300000020000001000000000.511.5 Ion 544.5, MSD1 544.5,Target Mass 543.5 +H Positive, EIC=544.2:545.2400000200000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.96922.5min1.51.97011.51.7281.85111.51.9361.9361.7281.849mAU2.1062.15522.5min2.10522.0062.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.73 0.02 4.24 2.69 0.37 233 1.85 0.02 1.49 0.85 0.13 544 1.94 0.02 1131.43 857.11 99.41 544 2.11 0.01 0.14 0.16 0.01 233 2.15 0.02 0.81 0.72 0.07 105 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.73 0.04 0.79 0.24 0.08 233 1.85 0.02 1.53 0.92 0.16 233 1.94 0.02 980.55 742.90 99.75 544 2.11 0.01 0.14 0.16 0.01 233 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|LCMS-03 12/8/2017 12:06:31 ZLJ_587Page1 of4MS Report from Instrument: LCMS-03 1.97 0.06 13019488.00 3305349.00 100.00 544LCMS-03 12/8/2017 12:06:31 ZLJ_587Page2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.97 <<<< POSITIVE SPECTRA >>>> ES-API Positive500000544.1546.1545.14000003000002000001000000100200300400500600700800900m/zLCMS-03 12/8/2017 12:06:31 ZLJ_587Page3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 12/8/2017 12:06:31 ZLJ_587Page4 of4
