Data File D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.DSample Name: CPK2015-914-05063=====================================================================Acq. Operator   : Yang Qian(LCMS-02)             Seq. Line :  50Acq. Instrument : HY-LCMS-02                      Location : P2-F-01Injection Date  : 9/15/2015 3:45:10 PM                 Inj :   1                                                Inj Volume : 3.000 µlAcq. Method     : D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\100-1000MS+3MIN-                  1.5_(0.02%FA).MLast changed    : 9/15/2015 11:13:01 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150911\\20150911 2015-09-11 09-13-22\\100-1500MS+3MIN_                  1.5(0.02%FA).M (Sequence Method)Last changed    : 9/15/2015 4:46:18 PM by Yang Qian(LCMS-02)                  (modified after loading)Method Info     : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No      : HY-10214 Batch#05063                  A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.D) 2.084 1.562 1.777 2.186mAU14001200100080060040020000.51 2.3521.522.53min =====================================================================                         Area Percent Report                         ===================================================================== Sorted By             :      SignalMultiplier            :      1.0000Dilution              :      1.0000Do not use Multiplier & Dilution Factor with ISTDs  Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type  Width     Area      Height     Area    #   [min]        [min]   [mAU*s]     [mAU]        %----|-------|----|-------|----------|----------|--------|   1   1.562 MM    0.0453    4.11423    1.51270   0.0953   2   1.777 MM    0.0448    9.26160    3.44908   0.2145   3   2.084 MF    0.0462 4293.160 1550.22510  99.4525   4   2.186 FM    0.0200    5.65672    4.70747   0.1310   5   2.352 MM    0.0548    4.60763    1.40075   0.1067 Totals :                  4317.53179 1561.29511  =====================================================================                          *** End of Report ***HY-LCMS-02 9/15/2015 4:46:19 PM Yang Qian(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.DSample Name: CPK2015-914-05063=====================================================================Acq. Operator   : Yang Qian(LCMS-02)             Seq. Line :  50Acq. Instrument : HY-LCMS-02                      Location : P2-F-01Injection Date  : 9/15/2015 3:45:10 PM                 Inj :   1                                                Inj Volume : 3.000 µlAcq. Method     : D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\100-1000MS+3MIN-                  1.5_(0.02%FA).MLast changed    : 9/15/2015 11:13:01 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150911\\20150911 2015-09-11 09-13-22\\100-1500MS+3MIN_                  1.5(0.02%FA).M (Sequence Method)Last changed    : 9/15/2015 4:47:13 PM by Yang Qian(LCMS-02)                  (modified after loading)Method Info     : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No      : HY-10214 Batch#05063                  A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.D)    ES-API, Pos, Sc 2.08850000040000030000020000010000000.511.522.53min HY-LCMS-02 9/15/2015 4:47:14 PM Yang Qian(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.DSample Name: CPK2015-914-05063MS Signal: MSD1 TIC, MS File,  ES-API, Pos, Scan, Frag: 50    Spectra averaged over upper half of peaks.    Noise Cutoff: 1000 counts.    Reportable Ion Abundance: > 10%.  Retention                   Mol. WeightTime (MS)      MS Area      or Ion    2.088       2732604       466.20 I                             465.20 I*MSD1 SPC, time=2.072:2.108 of D:\\AGLIENT 1260\\DATA\\20150915\\20150915 2015-09-15 11-13-01\\CPK2015-914-05063.D    ES-API100806040200100200300400500600700800900m/z 466.2 465.2Max: 357440                          *** End of Report ***HY-LCMS-02 9/15/2015 4:47:14 PM Yang Qian(LCMS-02)Page 2 of 2