MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-O11-WJ4.D Tgt Mass (EZX): 288.00 Injection Date : 11 Oct 16 10:24 am +0800 Seq. Line : 0 Sample Name : BIZ2016-O11-WJ4 Location : P1-B-09 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-N0822 Batch#22013 Easy-Access Method: '1-POS-3MIN' 288.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C *DAD1 B, Sig=214,4 Ref=off mAU1250100075025000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7060000500004000030000200001000000.511.5 Ion 2, MSD1 2,Target Mass 288 +H Positive, EIC=288.7:2.7 1200010000800060004000200000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min22.5min1.51.6982.2025002.04022.0412.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.70 0.03 5.32 -0.03 0.27 233 2.04 0.02 1942.91 1673. 99. 271 2.20 0.02 1.72 1.69 0.09 233HY-LCMS-02 10/11/2016 10:38:56 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 2.04 <<<< POSITIVE SPECTRA >>>> ES-API Positive600050004000 141.1 159.13000200010000200300400500600700800900m/z 233.3 271.1 221.1 272.2 290.2 247.3 2.2HY-LCMS-02 10/11/2016 10:38:56 KFF(LCMS-02)Page 2 of 2
