MS Report File ..0628 2016-06-28 10-42-34\\BIZ2016-628-WJ13.D Tgt Mass (CHM): Injection Date : 28 Jun 16 2:52 pm +0800 Seq. Line : 41 Sample Name : BIZ2016-628-WJ13 Location : P1-D-09 Acq. Operator : Su Xiao Ying(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\Aglient 1260\\Data\\20160628\\20160628 2016-06-28 10-42-34\\100-1000MS+3MIN- Analysis Method : D:\\AGLIENT 1260\\DATA\\20160628\\20160628 2016-06-28 10-42-34\\100-1000MS+3MIN- Catalog No : HY-16961 Batch#20834 A-RP-153 Method Info : HY-365_5HO1RS,M,A-RP-108,210nm,23min*DAD1 B, Sig=214,4 Ref=off 1.784mAU1500100050000.5*DAD1 C, Sig=254,4 Ref=off mAU20001.6772.1692.5901.6772.1132.2551.5692.3592.78511.51.78522.5min*2.3582.5901.5692.07700.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 501500001000005000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 0.050-0.050.5 Integration Results for DAD1 B, Sig=214,4 Ref=off-0.111.51.51.52.1522.2482.786100021.72.5min*22.5min22.5min RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.57 0.02 2.07 2.30 0.06 1.68 0.02 6. 4.93 0.18 1.78 0.03 3707.75 2166.85 98. 2.11 0.02 4.04 4.21 0.11 2.17 0.01 7.12 8.96 0.19 2.26 0.02 6.19 4.77 0.16 2.36 0.02 3.32 2.92 0.09 2.59 0.01 8.11 9.44 0.22 2.79 0.03 13.50 8.67 0.36 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.57 0.02 3.88 3. 0.07 1.68 0.03 13.53 8.47 0.23 1.78 0.03 5742.37 3168.63 98.58 2.08 0.02 5.67 0.28 0.10 2.15 0.01 9.25 -0.03 0.16HY-LCMS-02 6/28/2016 3:06:43 PM Su Xiao Ying(LCMS-02)Page 1 of 3
MS Report 2.25 0.02 3. 3.05 0.06 2.36 0.02 7.08 7.30 0.12 2.59 0.02 30.90 28.85 0.53 2.79 0.02 9.03 7.49 0.16HY-LCMS-02 6/28/2016 3:06:43 PM Su Xiao Ying(LCMS-02)Page 2 of 3
MS ReportRet. Time: 1.79 <<<< POSITIVE SPECTRA >>>> ES-API Positive 315.65000040000300002000010000 631.20200400600m/zHY-LCMS-02 6/28/2016 3:06:43 PM Su Xiao Ying(LCMS-02)Page 3 of 3